[1,2,4]三唑并[1,5-a]喹喔啉-4-醇合成路线 (共 3 条)
反应条件
copper(I) oxide in diethylene glycol T=135°C; 13 h;
参考文献
Catarzi, Daniela; Cecchi, Lucia; Colotta, Vittoria; Filacchioni, Guido; Melani, Fabrizio
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 5 p. 1161 - 1163
反应条件
1: 12 percent / triethylamine / benzene / 8 h 2: 70 percent / iron (powder), glacial acetic acid / 1 h / 90 °C 3: 90 percent / 0.6M aq. sodium hydroxide / ethanol / 3 h / Heating 4: 75 percent / cuprous oxide / bis-(2-hydroxy-ethyl) ether / 13 h / 135 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1161 - 1163
反应条件
1: 70 percent / iron (powder), glacial acetic acid / 1 h / 90 °C 2: 90 percent / 0.6M aq. sodium hydroxide / ethanol / 3 h / Heating 3: 75 percent / cuprous oxide / bis-(2-hydroxy-ethyl) ether / 13 h / 135 °C View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 29, # 5 p. 1161 - 1163