sodium hydrogencarbonate in N,N-dimethyl-formamide T=25°C; 19 h;

sulfuric acid 20 h; Heating / reflux;

1: carbon dioxide With [Au(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)hydroxide]; potassium hydroxide in tetrahydrofuran T=20°C; P=1125.11 Torr; 0.25 h; 2: isoxazole acid in tetrahydrofuran T=20°C; P=1125.11 Torr; 12 h; 3: methyl iodide in tetrahydrofuran regioselective reaction;

triethylamine in diethyl ether

暂无反应条件数据

diisobutylaluminium hydride in dichloromethane T=-78°C; 1 h;

in dimethyl sulfoxide 0.0833333 h; Heating;