2-叔丁基-6-羟基-4H-色烯-4-酮合成路线 （共 6 条）
反应条件
trifluorormethanesulfonic acid; hydroquinone in water
参考文献
Polaroid Corporation
Patent: US5354873 A1, 1994 ;
反应条件
hydroquinone in water
参考文献
Polaroid Corporation
Patent: US5919950 A1, 1999 ;
反应条件
sodium hydroxide in 1,4-dioxane T=60°C;
参考文献
Nussbaumer, Peter; Lehr, Philipp; Billich, Andreas
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4310 - 4320
反应条件
1: With formic acid T=100°C; 1 h; 2: With hydrogenchloride T=100°C; 1 h;
参考文献
Nussbaumer, Peter; Lehr, Philipp; Billich, Andreas
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4310 - 4320
反应条件
1.1: pyridine / 18 h / 20 °C 2.1: NaH / dimethylformamide / 2 h / 0 - 5 °C 3.1: formic acid / 1 h / 100 °C 3.2: aq. HCl / 1 h / 100 °C View Scheme
参考文献
Nussbaumer, Peter; Lehr, Philipp; Billich, Andreas
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4310 - 4320
反应条件
1.1: NaH / dimethylformamide / 2 h / 0 - 5 °C 2.1: formic acid / 1 h / 100 °C 2.2: aq. HCl / 1 h / 100 °C View Scheme
参考文献
Nussbaumer, Peter; Lehr, Philipp; Billich, Andreas
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4310 - 4320
