2-(2,2-二甲氧基乙基)苯甲酰胺合成路线 （共 15 条）
反应条件
sodium tris(acetoxy)borohydride in acetic acid
T=20 - 100°C; 2.5 h;
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
反应条件
1: 83 percent / NaBH(OAc)3 / acetic acid / 19 h / 20 - 50 °C
2: 98 percent / H2 / Pd/C / methanol / 20 h / 2585.74 Torr
3: 49 percent / K2CO3 / dimethylformamide / 20 °C
View Scheme
参考文献
Coe, Jotham W.; Vetelino, Michael G.; Bradlee, Michael J.
Tetrahedron Letters, 1996 , vol. 37, # 34 p. 6045 - 6048
反应条件
1: 83 percent / NaBH(OAc)3 / acetic acid / 19 h / 20 - 50 °C
2: 98 percent / H2 / Pd/C / methanol / 20 h / 2585.74 Torr
View Scheme
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
反应条件
sodium tris(acetoxy)borohydride in acetic acid
T=20 - 60°C;
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
反应条件
1: 83 percent / NaBH(OAc)3 / acetic acid / 19 h / 20 - 50 °C
2: 98 percent / H2 / Pd/C / methanol / 20 h / 2585.74 Torr
3: 97 percent / K2CO3 / dimethylformamide / 5 h / 20 - 50 °C
View Scheme
参考文献
Faul, Margaret M.; Grutsch, John L.; Kobierski, Michael E.; Kopach, Michael E.; Krumrich, Christine A.; Staszak, Michael A.; Udodong, Uko; Vicenzi, Jeffrey T.; Sullivan, Kevin A.
Tetrahedron, 2003 , vol. 59, # 36 p. 7215 - 7229
