(4-氰基亚苄基)-氨基甲酸叔丁酯合成路线 （共 11 条）
反应条件
in toluene 17 h; Heating;
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
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Vidal, Joelle; Damestoy, Stephanie; Guy, Laure; Hannachi, Jean-Christophe; Aubry, Andre; Collet, Andre
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1691 - 1709
反应条件
1: 92 percent / diethyl ether 2: 75 percent / toluene / 17 h / Heating View Scheme
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
反应条件
1: formic acid / methanol; water 2: potassium carbonate / dichloromethane; water / 4 h / 20 °C View Scheme
参考文献
Best, Daniel; Kujawa, Szymon; Lam, Hon Wai
Journal of the American Chemical Society, 2012 , vol. 134, # 44 p. 18193 - 18196
反应条件
1: formic acid / methanol; water 2: potassium carbonate / dichloromethane; water / 4 h / 20 °C View Scheme
参考文献
Tsai, Andy S.; Tauchert, Michael E.; Bergman, Robert G.; Ellman, Jonathan A.
Journal of the American Chemical Society, 2011 , vol. 133, # 5 p. 1248 - 1250
反应条件
1: ammonium hydroxide / ethanol; water / 18.58 h / -10 - 20 °C 2: water; methanol; formic acid / 72 h / 20 °C 3: caesium carbonate / dichloromethane / |Reflux View Scheme
参考文献
Best, Daniel; Kujawa, Szymon; Lam, Hon Wai
Journal of the American Chemical Society, 2012 , vol. 134, # 44 p. 18193 - 18196
反应条件
1: LiMCPBA / CH2Cl2 / 2 h / -78 °C 2: CD2Cl2 / -94 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 3, # 10 p. 1691 - 1709
反应条件
1: LiMCPBA / CH2Cl2 / 2 h / -78 °C 2: 35 percent / LiHMDS / tetrahydrofuran / -78 °C / 1.) 30 min, 2.) 30 min View Scheme
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
反应条件
Oxonereg;; potassium carbonate in chloroform; water T=0 - 4°C;
参考文献
Journal of Organic Chemistry, , vol. 58, # 18 p. 4791 - 4793
反应条件
LiMCPBA in dichloromethane T=-78°C; 2 h; Yield given;
参考文献
Vidal, Joelle; Damestoy, Stephanie; Guy, Laure; Hannachi, Jean-Christophe; Aubry, Andre; Collet, Andre
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1691 - 1709
反应条件
1: LiMCPBA / CH2Cl2 / 2 h / -78 °C
2: CD2Cl2 / -94 °C
3: toluene / 111 h / Heating
View Scheme
参考文献
Vidal, Joelle; Damestoy, Stephanie; Guy, Laure; Hannachi, Jean-Christophe; Aubry, Andre; Collet, Andre
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1691 - 1709
