N-叔丁氧羰基-3-(4-氰苯基)哑嗪合成路线 (共 28 条)
反应条件
in chloroform
T=-15°C; 1 h;
参考文献
Vidal, Joelle; Guy, Laure; Sterin, Sebastien; Collet, Andre
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4791 - 4793
反应条件
N-benzyl-trimethylammonium hydroxide
1.) MeOH, 30 min, 2.) CHCl3, -30 deg C, 1 h;
参考文献
Vidal, Joelle; Damestoy, Stephanie; Guy, Laure; Hannachi, Jean-Christophe; Aubry, Andre; Collet, Andre
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1691 - 1709
反应条件
1: n-butyllithium With zinc(II) chloride in diethyl ether; hexane
T=0°C; 0.5 h; Inert atmosphere;
2: N-(tert-butoxycarbonyl)-3-(4-cyanophenyl)-oxaziridine in diethyl ether; hexane
T=0°C; 0.666667 h; Inert atmosphere;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
in diethyl ether; hexane
T=0°C; 0.583333 h;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
in tetrahydrofuran; hexane
T=-78°C; 0.166667 h;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
in tetrahydrofuran; diethyl ether; hexane
T=0°C; 0.5 h;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
in diethyl ether; hexane
T=0°C; 0.5 h;
参考文献
Ghoraf, Mohammed; Vidal, Joelle
Tetrahedron Letters, 2008 , vol. 49, # 52 p. 7383 - 7385
反应条件
in chloroform-d1
T=19°C; other solvents, temperature; Product distribution;
参考文献
Vidal, Joelle; Damestoy, Stephanie; Guy, Laure; Hannachi, Jean-Christophe; Aubry, Andre; Collet, Andre
Chemistry - A European Journal, 1997 , vol. 3, # 10 p. 1691 - 1709