3-甲酰基酪醇alpha-乙酸酯合成路线 (共 2 条)
反应条件
hydrogenchloride in tetrahydrofuran 48 h; Ambient temperature;
参考文献
Maruyama; Kobayashi; Osuka
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 9 p. 2672 - 2681
反应条件
1: potassium carbonate; sodium iodide / N,N-dimethyl-formamide / 60 °C 2: diphenyl diselenide; dihydrogen peroxide / dichloromethane / 48 h / 20 °C 3: palladium 10 on activated carbon; hydrogen / ethyl acetate / 0.5 h / 20 °C / 760.05 Torr 4: methanol; ammonia / 1 h / 20 °C 5: hydrogenchloride / dichloromethane View Scheme
参考文献
Piersanti, Giovanni; Retini, Michele; Espartero, Jose L.; Madrona, Andres; Zappia, Giovanni
Tetrahedron Letters, 2011 , vol. 52, # 38 p. 4938 - 4940