1,1,2,3,3-五氯丙烷合成路线 （共 14 条）
反应条件
potassium hydroxide cis-trans-mixture;
参考文献
Prins
Patent: DE261689 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 1206
Full Text Show Details
Prins
Journal fuer Praktische Chemie (Leipzig), 1914 , vol. <2>89, p. 416
反应条件
sodium hydroxide in water
参考文献
Merck and Co., Inc.
Patent: US6369275 B1, 2002 ;
Location in patent: Page column 17-18 ;
反应条件
AIBMe; chlorine in tetrachloromethane
T=70°C; P=8517.48 Torr; 2.08333 h; Sealed tube; Time;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; FISH, Barry; LAITAR, David Stephen
Patent: WO2013/22677 A1, 2013 ;
Location in patent: Page/Page column 0066 ;
反应条件
AIBMe; chlorine
T=70°C; P=8517.48 Torr; 3.33333 h; Sealed tube;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; FISH, Barry; LAITAR, David Stephen
Patent: WO2013/22677 A1, 2013 ;
Location in patent: Page/Page column 0064; 0065 ;
反应条件
chlorine; 1,1'-azobis (cyclohexanecarbonitrile) in tetrachloromethane
T=70°C; P=6723.1 Torr; 5.58333 h; Inert atmosphere; Product distribution / selectivity;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 19-20 ;
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile
T=55 - 60°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile
T=55 - 60°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
sulfuryl dichloride; 2,2'-azo-bisisobutyronitrile
T=55 - 60°C;
参考文献
DOW GLOBAL TECHNOLOGIES, LLC; TIRTOWIDJOJO, Max Markus; KRUPER, William J.; FISH, Barry; LAITAR, David Stephen
Patent: WO2012/166394 A1, 2012 ;
Location in patent: Page/Page column 18-19 ;
反应条件
aluminium trichloride
T=10 - 20°C;
参考文献
Prins
Patent: DE261689 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 11, p. 1206
Full Text Show Details
Prins
Journal fuer Praktische Chemie (Leipzig), 1914 , vol. <2>89, p. 416
反应条件
aluminium trichloride
参考文献
Heilbron; Heslop; Irving
Journal of the Chemical Society, 1936 , p. 784
Full Text Show Details
Prins; Engelhard
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 309
Full Text Show Details
Prins
Recueil des Travaux Chimiques des Pays-Bas, 1949 , vol. 68, p. 898,899
Recueil des Travaux Chimiques des Pays-Bas, 1953 , vol. 72, p. 253,256, 260
