3-(1H-咪唑-1-基甲基)-苯甲醇合成路线 (共 4 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Cozzi, Paolo; Carganico, Germano; Fusar, Domenico; Grossoni, Mauro; Menichincheri, Maria; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 20 p. 2964 - 2972
反应条件
1: NBS / CCl4 / 3 h / Heating 2: dimethylformamide / 5 h / Ambient temperature 3: 80 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Cozzi, Paolo; Carganico, Germano; Fusar, Domenico; Grossoni, Mauro; Menichincheri, Maria; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 20 p. 2964 - 2972
反应条件
1: dimethylformamide / 5 h / Ambient temperature 2: 80 percent / LiAlH4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Cozzi, Paolo; Carganico, Germano; Fusar, Domenico; Grossoni, Mauro; Menichincheri, Maria; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 20 p. 2964 - 2972
反应条件
oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-60 - -50°C; 0.5 h;
参考文献
Cozzi, Paolo; Carganico, Germano; Fusar, Domenico; Grossoni, Mauro; Menichincheri, Maria; et al.
Journal of Medicinal Chemistry, 1993 , vol. 36, # 20 p. 2964 - 2972