3-环己烯-1-羧酸乙酯合成路线 （共 19 条）
反应条件
1.)thionyl chloride 2.)pyridine; Multistep reaction;
参考文献
Journal of Physical Chemistry, , vol. 87, # 3 p. 408 - 417
反应条件
1: With water; sodium hydroxide in ethanol T=20°C; 16 h; 2: With hydrogenchloride in ethanol; water Product distribution / selectivity;
参考文献
Daiichi Sankyo Company, Limited
Patent: EP2368870 A1, 2011 ;
Location in patent: Page/Page column 13 ;
EP 2368870 A1
反应条件
IrradiationArrhenius parameters, different threshold energies; Product distributionThermodynamic data;
参考文献
Setser, D. W.; Nguyen, Hanh H.; Danen, Wayne C.
Journal of Physical Chemistry, 1983 , vol. 87, # 3 p. 408 - 417
反应条件
1: sodium hydroxide; water / ethanol / 16 h / 20 °C 2: water; acetone / 23 h / 10 - 50 °C 3: hydrogenchloride / water; tert-butyl methyl ether / 1 h / 20 °C / pH 1 View Scheme
参考文献
EP2368870 A1, ;
EP 2368870 A1
反应条件
magnesium; palladium on activated charcoal in methanol Ambient temperature;
参考文献
Olah, George A.; Prakash, G. K. Surya; Arvanaghi, Massoud; Bruce, Mark R.
Angewandte Chemie, 1981 , vol. 93, # 1 p. 107
反应条件
IrradiationArrhenius parameters, different threshold energies; Product distributionThermodynamic data;
参考文献
Setser, D. W.; Nguyen, Hanh H.; Danen, Wayne C.
Journal of Physical Chemistry, 1983 , vol. 87, # 3 p. 408 - 417
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Wilcox,C.F.; Chibber,S.S.
Journal of Organic Chemistry, 1962 , vol. 27, p. 2332 - 2338
反应条件
1: LiAlH4 / diethyl ether / Heating 2: NaNO2, H2SO4 / H2O / -10 °C 3: benzene / 10 h / Irradiation View Scheme
参考文献
Nouguier,R.; Surzur,J.-M.
Bulletin de la Societe Chimique de France, 1973 , p. 2399 - 2403
反应条件
IrradiationArrhenius parameters, different threshold energies; Product distributionThermodynamic data;
参考文献
Setser, D. W.; Nguyen, Hanh H.; Danen, Wayne C.
Journal of Physical Chemistry, 1983 , vol. 87, # 3 p. 408 - 417
