1: 50 percent / hexane; diethyl ether / -20 - 0 °C
2: 0.5 g / benzene / 150 h / 120 °C
View Scheme
参考文献
Vasisht, S. K.; Kaur, Tripat P.; Usha, K.; Kaushal, Jyotsna; Bandhu, Kavita
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 107, # 1-4 p. 189 - 196
in hexane
byproducts: LiCl, SnCl2; To a soln. of Li-compd. (-80°C) SnCl4 is dropwise added (under vac., absence of air and moisture).; NMR, fractional distn.;
参考文献
Verma, P. K.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1991 , vol. 605, p. 131 - 136
Vasisht, S. K.; Kaur, Tripat P.; Usha, K.; Kaushal, Jyotsna; Bandhu, Kavita
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 107, # 1-4 p. 189 - 196
in hexane
byproducts: LiCl, SnCl2; To a soln. of Li-compd. (-80°C) SnCl4 is dropwise added (under vac., absence of air and moisture).; NMR, fractional distn.;
参考文献
Verma, P. K.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1991 , vol. 605, p. 131 - 136
