2-甲氧基-6-戊基苯酚合成路线 (共 15 条)
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Koenig, Wilfried A.; Faasch, Holger; Heitsch, Holger; Colberg, Cornelia; Hausen, Bjoern M.
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1993 , vol. 48, # 3 p. 387 - 393
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
参考文献
Davis, Christopher J.; Hurst, Timothy E.; Jacob, Aouregan M.; Moody, Christopher J.
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4414 - 4422
反应条件
lithium hydroxide hydrate in N,N-dimethyl-formamide T=20°C; Cooling with iceInert atmosphere;
参考文献
Bhattacharya, Asish K.; Kaur, Tanpreet; Ganesh, Krishna N.
Synthesis, 2010 , # 7 art. no. Z26109SS, p. 1141 - 1144
反应条件
1: 96 percent / dimethylformamide / 0.42 h / 180 °C / microwave irradiation 2: 80 percent / H2 / Pd/C / ethyl acetate / 17 h View Scheme
参考文献
Davis, Christopher J.; Moody, Christopher J.
Synlett, 2002 , # 11 p. 1874 - 1876
反应条件
1: 49 percent / triphenylphosphine; diisopropyl azodicarboxylate / toluene / 24 h / 20 °C 2: 96 percent / dimethylformamide / 0.42 h / 180 °C / microwave irradiation 3: 80 percent / H2 / Pd/C / ethyl acetate / 17 h View Scheme
参考文献
Mabic; Vaysse; Benezra; Lepoittevin
Synthesis, 1999 , # 7 p. 1127 - 1134
反应条件
sodium; butan-1-ol T=80 - 90°C; 1 h;
参考文献
Wu, Li-Qiang; Yang, Chun-Guang; Yang, Li-Ming; Yang, Li-Juan
Journal of the Chinese Chemical Society (Taipei, Taiwan), 2009 , vol. 56, # 1 p. 47 - 50
反应条件
1.1: Mg / tetrahydrofuran 1.2: tetrahydrofuran / 0 - 20 °C 2.1: H2 / 5percent Pd/C / methanol / 20 °C View Scheme
参考文献
Arogba, Sunday S.
Organic Preparations and Procedures International, 1991 , vol. 23, # 5 p. 639 - 644
反应条件
sodium hydroxide in ethanol 12 h; Heating; Yield given;
参考文献
Mabic; Vaysse; Benezra; Lepoittevin
Synthesis, 1999 , # 7 p. 1127 - 1134
反应条件
1: 1.) s-BuLi, TMEDA, 2.) Br2 / 1.) Et2O, 2.) Et2O 3: NaOH / ethanol / 12 h / Heating View Scheme
参考文献
Mabic; Vaysse; Benezra; Lepoittevin
Synthesis, 1999 , # 7 p. 1127 - 1134
反应条件
2: NaOH / ethanol / 12 h / Heating View Scheme
参考文献
Mabic; Vaysse; Benezra; Lepoittevin
Synthesis, 1999 , # 7 p. 1127 - 1134