3-(4-甲氧基苯甲酰)丙酸乙酯合成路线 （共 16 条）
反应条件
(PhCO)PdCl(PPh3)2*(CH2Cl2) in chloroform-d1 T=90 - 100°C; 24 h;
参考文献
Tetrahedron Letters, , vol. 30, # 47 p. 6541 - 6544
反应条件
2,2'-azo-bisisobutyronitrile; diMe-Imd-BH3 in acetonitrile T=80°C; P=60804.1 Torr; 4 h; Autoclave; chemoselective reaction;
参考文献
Organic Letters, , vol. 15, # 9 p. 2144 - 2147
反应条件
sulfuric acid in ethanol; water
反应条件
1: 3-chlorocarbonyl-propionic acid ethyl ester With aluminium trichloride in dichloromethane T=0°C; 0.25 h; 2: methoxybenzene in dichloromethane T=20°C; Friedel-Crafts acylation; 15 h;
参考文献
Imoto, Hiroshi; Matsumoto, Mitsuharu; Odaka, Hiroyuki; Sakamoto, Junichi; Kimura, Hiroyuki; Nonaka, Masami; Kiyota, Yutaka; Momose, Yu
Chemical and Pharmaceutical Bulletin, 2004 , vol. 52, # 1 p. 120 - 124
反应条件
sulfuric acid in benzene 14 h; Heating;
参考文献
Mahmoodi; Yousefi-Malekroudi
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 3 p. 365 - 368
反应条件
Cu(1,1,1,5,5,5-hexafluoroacetylacetonate)2 in o-di-fluorobenzene Heating;
参考文献
Huang, Dan; Yan, Ming; Zhao, Wei-Jie; Shen, Qi
Synthetic Communications, 2005 , vol. 35, # 5 p. 745 - 750
反应条件
toluene-4-sulfonic acid T=120°C; 0.5 h; microwave irradiation;
参考文献
Jacubert, Maud; Provot, Olivier; Peyrat, Jean-Francois; Hamze, Abdallah; Brion, Jean-Daniel; Alami, Mouad
Tetrahedron, 2010 , vol. 66, # 21 p. 3775 - 3787
反应条件
in N,N-dimethyl-formamide T=160°C; 6 h;
参考文献
Sangu, Kenichiro; Watanabe, Toru; Takaya, Jun; Iwasawa, Nobuharu
Synlett, 2007 , # 6 p. 929 - 933
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl acetamide; benzene T=60°C; 0.5 h; various co-solsents;
参考文献
Tamaru, Yoshinao; Ochiai, Hirofumi; Nakamura, Tatsuya; Tsubaki, Kazunori; Yoshida, Zen-ichi
Tetrahedron Letters, 1985 , vol. 26, # 45 p. 5559 - 5562
反应条件
1: aluminium chloride; carbon disulfide 2: hydrochloric acid View Scheme
参考文献
Journal of the American Chemical Society, , vol. 38, p. 1533
