2-(2-硝基苯基)乙醇合成路线 (共 40 条)
反应条件
nitric acid T=-15°C; Verseifung des entstandenen Acetats mit methylalkoholischer Salzsaeure;
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 45, p. 845,846
反应条件
tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide 3.6 h; Ambient temperatureelectroreduction; other nitroalkylbenzenes, var. supporting electrolites, solvents, and current conditions; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 51, # 16 p. 3143 - 3147
反应条件
sodium tetrahydroborate; aluminium trichloride
参考文献
Canadian Journal of Chemistry, , vol. 49, p. 2023 - 2028
反应条件
1: H2SO4 2: concentrated sulfuric acid; nitric acid / 0 °C / Kochen des Reaktionsprodukts mit methanol. HCl View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 53, p. 330,332
反应条件
nitric acid; urea 1.) from -12 deg C to -5 deg C, 20 min, 2.) reflux, 5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 10.1 p. 1556 - 1558
Zhurnal Organicheskoi Khimii, , vol. 30, # 10 p. 1478 - 1480
反应条件
T=-15°C; Verseifen der entstandenen Acetate mit methylalkoholischer Salzsaeure;
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 45, p. 845,846
Chemische Berichte, , vol. 62, p. 190
反应条件
1: 78 percent / calcium chloride; zinc powder / H2O / 0.5 h / Heating 2: 72 percent / NaHCO3 / dioxane 3: 63 percent / PBr3; pyridine / hexane 4: HCl View Scheme
参考文献
Minin, Patricia L.; Walton, John C.
Journal of Organic Chemistry, 2003 , vol. 68, # 7 p. 2960 - 2963
参考文献
Research Association for Utilization of Light Oil
Patent: US4937382 A1, 1990 ;
反应条件
N-methyl-pyrrolidine; selenium in tetrahydrofuran T=150°C; P=22800 Torr; 5 h;
参考文献
Nishiyama, Yutaka; Naitoh, Yoshitaka; Sonoda, Noboru
Synlett, 2004 , # 5 p. 886 - 888
参考文献
Sabetay; Tchang; Mintsou
Bulletin de la Societe Chimique de France, 1929 , vol. <4> 45, p. 846