tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide 3.6 h; Ambient temperatureelectroreduction; other nitroalkylbenzenes, var. supporting electrolites, solvents, and current conditions; Product distributionMechanism;

1: 97 percent / trifluoroacetic acid, dicyclohexylcarbodiimide, pyridine / benzene; dimethylsulfoxide / 2 h / Ambient temperature 2: 40 percent / hydrogen / PtO2 / methanol / 3 h / 760 Torr / Ambient temperature View Scheme

jones reagent in acetone 6 h; Ambient temperatureaddition at 0 deg C;

1: 97 percent / trifluoroacetic acid, dicyclohexylcarbodiimide, pyridine / benzene; dimethylsulfoxide / 2 h / Ambient temperature 2: 93 percent / aq. 31percent H2O2, aq. 24percent NaOH / methanol / 1 h / 10 °C / addition at -5 to 0 deg C 3: 53 percent / hydrogen / Pd/C / acetic anhydride / 760 Torr / Ambient temperature View Scheme

pyridine; dicyclohexyl-carbodiimide; trifluoroacetic acid in dimethyl sulfoxide; benzene 2 h; Ambient temperature;

hydrogen; palladium on activated charcoal in ethyl acetate 15 h; Ambient temperature;