反应条件
1.1: ozone / methanol; dichloromethane / -78 °C 1.2: 3 h / -78 - 20 °C / |Inert atmosphere 2.1: hydrogenchloride / tetrahydrofuran; water / 16 h / 20 °C 3.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C / |Schlenk technique; |Inert atmosphere 3.2: 1 h / 20 °C / |Schlenk technique; |Inert atmosphere View Scheme
参考文献
UNIVERSITY OF BRISTOL; AGGARWAL, Varinder, Kumar; COULTHARD, Mark, Graeme; ERB, William
Patent: WO2013/186550 A1, 2013 ;
