1,3,5-三(4-碘苯基)苯合成路线 （共 7 条）
反应条件
boron sulfonic acid in neat liquid T=100°C; 6 h; Green chemistry;
参考文献
Safaei, Hamid Reza; Davoodi, Mansooreh; Shekouhy, Mohsen
Synthetic Communications, 2013 , vol. 43, # 16 p. 2178 - 2190
反应条件
iodine; sodium hydrogencarbonate; sodium thiosulfate; acetic acid; sulfuric acid in toluene
参考文献
Bando Chemical Industries, Ltd.
Patent: EP1826837 A1, 2007 ;
反应条件
iodine cloride in dichloromethane T=0°C;
参考文献
Moon, Kyung-Soo; Lee, Eunji; Lee, Myongsoo
Chemical Communications, 2008 , # 26 p. 3061 - 3063
反应条件
bis(allyl)-ruthenium(IV) dimer in methanol; water T=75°C; 0.75 h;
参考文献
Cadierno, Victorio; Garcia-Garrido, Sergio E.; Gimeno, Jose
Journal of the American Chemical Society, 2006 , vol. 128, # 47 p. 15094 - 15095
反应条件
hydrogenchloride; trimethyl orthoformate in chloroform T=0 - 20°C;
参考文献
Yu; Lindsey
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7402 - 7419
反应条件
1: 97 percent / CuI; Pd(PPh3)2Cl2; PPh3 / Et3N / tetrahydrofuran / 5 h / 20 °C
2: 85 percent / K2CO3 / methanol; tetrahydrofuran / 3 h / 20 °C
View Scheme
参考文献
Simpson, Christopher D.; Mattersteig, Gunter; Martin, Kai; Gherghel, Lileta; Bauer, Roland E.; Raeder, Hans Joachim; Muellen, Klaus
Journal of the American Chemical Society, 2004 , vol. 126, # 10 p. 3139 - 3147
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium carbonate in tetrahydrofuran; water; toluene
T=110°C; Suzuki coupling; 24 h; Inert atmosphere;
参考文献
Dash, Barada Prasanna; Satapathy, Rashmirekha; Gaillard, Elizabeth R.; Maguire, John A.; Hosmane, Narayan S.
Journal of the American Chemical Society, 2010 , vol. 132, # 18 p. 6578 - 6587
