N-(2-甲酰基-5,8-二氧代-5,8-二氢喹啉-7-基)乙酰胺合成路线 （共 6 条）
反应条件
selenium(IV) oxide in 1,4-dioxane; water 9 h; Heating;
参考文献
Seradj, Hassan; Cai, Wen; Erasga, Noe O.; Chenault, Darrell V.; Knuckles, Kathryn A.; Ragains, Justin R.; Behforouz, Mohammad
Organic Letters, 2004 , vol. 6, # 4 p. 473 - 476
反应条件
1.1: H2; HCl / Pd/C / H2O / 15 h / 20 °C / 1551.44 Torr 2.1: NaOAc; Ma2CO3 / 2.5 h / 0 - 20 °C 2.2: methanol / 0.5 h / Heating 3.1: 71 percent / K2Cr2O7; AcOH; H2O / 24 h / 20 °C 4.1: 91 percent / SeO2 / dioxane; H2O / Heating View Scheme
参考文献
Behforouz, Mohammad; Haddad, Jalal; Cai, Wen; Arnold, Macklin B.; Mohammadi, Farahnaz; Sousa, Aron C.; Horn, Mark A.
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6552 - 6555
反应条件
1: 72 percent / HNO3, H2SO4 / 2 h / 0 - 5 °C 2: 98 percent / H2, aq. HCl / Pd-C / 15 h / 1551.4 Torr 3: 85 percent / NaOAc, Na2SO3 / H2O / 3.25 h 4: 60 percent / aq. K2Cr2O7, AcOH / 15 h 5: 91 percent / SeO2 View Scheme
参考文献
Behforouz, Mohammad; Haddad, Jalal; Cai, Wen; Arnold, Macklin B.; Mohammadi, Farahnaz; Sousa, Aron C.; Horn, Mark A.
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6552 - 6555
反应条件
1: 71 percent / K2Cr2O7; AcOH; H2O / 24 h / 20 °C 2: 91 percent / SeO2 / dioxane; H2O / Heating View Scheme
参考文献
Behforouz, Mohammad; Haddad, Jalal; Cai, Wen; Arnold, Macklin B.; Mohammadi, Farahnaz; Sousa, Aron C.; Horn, Mark A.
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6552 - 6555
反应条件
1.1: NaOAc; Ma2CO3 / 2.5 h / 0 - 20 °C 1.2: methanol / 0.5 h / Heating 2.1: 71 percent / K2Cr2O7; AcOH; H2O / 24 h / 20 °C 3.1: 91 percent / SeO2 / dioxane; H2O / Heating View Scheme
参考文献
Seradj, Hassan; Cai, Wen; Erasga, Noe O.; Chenault, Darrell V.; Knuckles, Kathryn A.; Ragains, Justin R.; Behforouz, Mohammad
Organic Letters, 2004 , vol. 6, # 4 p. 473 - 476
反应条件
1: 60 percent / aq. K2Cr2O7, AcOH / 15 h 2: 91 percent / SeO2 View Scheme
参考文献
Behforouz, Mohammad; Haddad, Jalal; Cai, Wen; Arnold, Macklin B.; Mohammadi, Farahnaz; Sousa, Aron C.; Horn, Mark A.
Journal of Organic Chemistry, 1996 , vol. 61, # 19 p. 6552 - 6555
