3-甲基-6-硝基-4H-1,3-苯并恶嗪-2-酮合成路线 (共 7 条)
反应条件
sulfuric acid; nitric acid in acetic acid 1.5 h; Ambient temperature;
参考文献
Kitson, Trevor M.; Freeman, Graham H.
Bioorganic Chemistry, 1993 , vol. 21, # 3 p. 354 - 365
反应条件
2,3-dimethyl aniline in dichloromethane; toluene 0.5 h; Heating;
参考文献
Mindl, Jaromir; Hrabik, Oldrich; Sterba, Vojeslav; Kavalek, Jaromir
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 8 p. 1262 - 1272
反应条件
1: NaBH4 / ethanol 2: 23 percent / N,N-dimethylaniline / toluene / Ambient temperature 3: 80 percent / H2SO4, HNO3 / acetic acid / 1.5 h / Ambient temperature View Scheme
参考文献
Kitson, Trevor M.; Freeman, Graham H.
Bioorganic Chemistry, 1993 , vol. 21, # 3 p. 354 - 365
反应条件
1: 23 percent / N,N-dimethylaniline / toluene / Ambient temperature 2: 80 percent / H2SO4, HNO3 / acetic acid / 1.5 h / Ambient temperature View Scheme
参考文献
Kitson, Trevor M.; Freeman, Graham H.
Bioorganic Chemistry, 1993 , vol. 21, # 3 p. 354 - 365
反应条件
1: 83 percent / H2O / Ambient temperature 2: NaBH4 / ethanol 3: 23 percent / N,N-dimethylaniline / toluene / Ambient temperature 4: 80 percent / H2SO4, HNO3 / acetic acid / 1.5 h / Ambient temperature View Scheme
参考文献
Kitson, Trevor M.; Freeman, Graham H.
Bioorganic Chemistry, 1993 , vol. 21, # 3 p. 354 - 365
反应条件
in 1,4-dioxane 1 h; Heating;
参考文献
Mindl, Jaromir; Hrabik, Oldrich; Sterba, Vojeslav; Kavalek, Jaromir
Collection of Czechoslovak Chemical Communications, 2000 , vol. 65, # 8 p. 1262 - 1272
反应条件
water in methanol pH=6.70 - 10.30; Kinetics;
参考文献
Sterba, Vojeslav; Hrabik, Oldrich; Kavalek, Jaromir; Mindl, Jaromir; Williams, Andrew
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 2 p. 415 - 421