1,1,1,3,3,3-六氟-2-甲基-2-丙醇合成路线 （共 7 条）
反应条件
methyllithium in diethyl ether T=0°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 34, # 5 p. 1278 - 1281
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , # 4 p. 647 - 653
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 4 p. 686 - 692
反应条件
magnesium 1.) Et2O, -15 deg C to 15 deg C, 2.) Et2O, -15 deg C, then 12 h room temp.; Yield given. Multistep reaction;
参考文献
Journal fur Praktische Chemie - Chemiker - Zeitung, , vol. 339, # 5 p. 479 - 481
反应条件
chlorine
9 h; Irradiation;
参考文献
Dear,R.E.A.
Synthesis, 1970 , p. 361 - 362
反应条件
NaF
in presence of excess NaF, 25°C, 1 h;
参考文献
Kitazume; Shreeve
Journal of the American Chemical Society, 1977 , vol. 99, p. 4194
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Kitazume, T.; Shreeve, J. M.
J. Inorg. Chem., 1978 , vol. 17, p. 2173 - 2176
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Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.2, page 1 - 48
参考文献
Dear,R.E.A. et al.
Tetrahedron, 1971 , vol. 27, p. 3345 - 3355
反应条件
NaF
with excess of NaF at 25°C, 1 h;
参考文献
Kitazume; Shreeve
Inorganic Chemistry, 1978 , vol. 17, p. 2173
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Gmelin Handbook: F: PerFHalOrg.SVol.3, 6.2.3.2, page 121 - 136
