N-正丁基邻苯二甲酰亚胺合成路线 （共 47 条）
反应条件
benzene und Erwaermen der erhaltenen N-Butyl-N-methyl-phthalamidsaeure mit Thionylchlorid und Erhitzen des Reaktionsprodukts auf 250grad bei 1-2 Torr;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 18, p. 80,83
反应条件
potassium hydroxide; water; dihydrogen peroxide
参考文献
Journal of the Chemical Society, , p. 709,717
反应条件
hydrogenchloride; water
参考文献
Journal of the Chemical Society, , p. 709,717
反应条件
potassium carbonate; formamide 1) 210 deg C; 2) DMFA, boiling; Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 23, # 5 p. 981 - 983
Zhurnal Organicheskoi Khimii, , vol. 23, # 5 p. 1086 - 1089
反应条件
hexamethylene diamine T=170 - 200°C; Yield given;
参考文献
Ganin, E. V.; Makarov, V. F.; Nikitin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 981 - 983
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 1086 - 1089
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran
T=25°C; Inert atmosphere;
参考文献
Das, Shoubhik; Addis, Daniele; Knoepke, Leif R.; Bentrup, Ursula; Junge, Kathrin; Brueckner, Angelika; Beller, Matthias
Angewandte Chemie - International Edition, 2011 , vol. 50, # 39 p. 9180 - 9184
反应条件
1: lithium alanate; diethyl ether
2: methanol
View Scheme
参考文献
Rice et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 884,888
