N1-(特戊酰氧基)甲基-N2-(二甲基氨基)亚甲基9-脱氮鸟嘌呤合成路线 （共 8 条）
参考文献
Taylor; Young; Ward
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4595 - 4598
反应条件
1: 91 percent / CH2Cl2 / 5 h / Ambient temperature 2: 60 percent / NaH / dimethylformamide / 1.) r.t., 1 h, 2.) r.t., 12 h 3: 86 percent / dimethylformamide / 12 h / Ambient temperature 4: 94 percent / aq. Na2S2O4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Taylor; Young; Ward
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4595 - 4598
反应条件
1: 60 percent / NaH / dimethylformamide / 1.) r.t., 1 h, 2.) r.t., 12 h 2: 86 percent / dimethylformamide / 12 h / Ambient temperature 3: 94 percent / aq. Na2S2O4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Taylor; Young; Ward
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4595 - 4598
反应条件
1: 86 percent / dimethylformamide / 12 h / Ambient temperature 2: 94 percent / aq. Na2S2O4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Taylor; Young; Ward
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4595 - 4598
反应条件
1: 89 percent / conc. HNO3, conc. H2SO4 / 3 h / Ambient temperature 2: 91 percent / CH2Cl2 / 5 h / Ambient temperature 3: 60 percent / NaH / dimethylformamide / 1.) r.t., 1 h, 2.) r.t., 12 h 4: 86 percent / dimethylformamide / 12 h / Ambient temperature 5: 94 percent / aq. Na2S2O4 / tetrahydrofuran / 1 h / Ambient temperature View Scheme
参考文献
Taylor, Edward C.; Young, Wendy B.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7947 - 7952
反应条件
1: 1) NaH 2: 86 percent / dimethylformamide / Ambient temperature 3: 94 percent / Na2S2O4 View Scheme
参考文献
Taylor; Young; Ward
Tetrahedron Letters, 1993 , vol. 34, # 29 p. 4595 - 4598
反应条件
sodium hydroxide in ethanol
参考文献
Taylor, Edward C.; Young, Wendy B.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7947 - 7952
反应条件
sodium hydride in N,N-dimethyl-formamide
1.) 0 deg C, 20 min, 2.) 0 deg C, 2 h;
参考文献
Taylor, Edward C.; Young, Wendy B.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7947 - 7952
