1,3-二-叔丁基-2-甲氧基苯合成路线 (共 10 条)
反应条件
barium dihydroxide in N,N-dimethyl-formamide
参考文献
Diemer, Vincent; Chaumeil, Helene; Defoin, Albert; Fort, Alain; Boeglin, Alex; Carre, Christiane
European Journal of Organic Chemistry, 2008 , # 10 p. 1767 - 1776
反应条件
barium dihydroxide in N,N-dimethyl-formamide Ambient temperature;
参考文献
Mase, Nobuyuki; Watanabe, Yoshihiko; Ueno, Yoshio; Toru, Takeshi
Journal of Organic Chemistry, 1997 , vol. 62, # 22 p. 7794 - 7800
反应条件
lithium in tetrahydrofuran; tert-butyl alcohol T=70°C; 8 h;
参考文献
Knorr, Rudolf; Rossmann, Eva Christine; Knittl, Monika
Synthesis, 2010 , # 13 art. no. C01110SS, p. 2124 - 2128
反应条件
(i) KOtBu, tBuOH, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Kornblum,N.; Seltzer,R.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3668 - 3671
反应条件
lithium; ethylenediamine in tetrahydrofuran T=-10°C; 0.5 h;
参考文献
Shindo, Takeyuki; Fukuyama, Yasuaki; Sugai, Takeshi
Synthesis, 2004 , # 5 p. 692 - 700
反应条件
1: 1,3-Di-tert-butyl-2-methoxy benzene With 4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=20°C; 1.55 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran 0.5 h; Heating;
参考文献
Synthesis, , # 13 art. no. C01110SS, p. 2124 - 2128
反应条件
1: 1,3-Di-tert-butyl-2-methoxy benzene With 4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran T=20°C; 1.55 h; Inert atmosphere; 2: carbon dioxide in tetrahydrofuran 0.5 h; Heating;
参考文献
Synthesis, , # 13 art. no. C01110SS, p. 2124 - 2128
反应条件
4,4'-di-tert-butylbiphenyl; lithium Acidic conditions;
参考文献
Knorr, Rudolf; Rossmann, Eva Christine; Knittl, Monika
Synthesis, 2010 , # 13 art. no. C01110SS, p. 2124 - 2128
反应条件
N-bromosuccinmide in acetonitrile 48 h;
参考文献
European Journal of Organic Chemistry, , # 10 p. 1767 - 1776
反应条件
sodium nitrite in acetic acid
参考文献
Vol'eva, V. B.; Komissarova, N. L.; Belostotskaya, I. S.; Grishina, E. A.; Ershov, V. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 10 p. 2088 - 2090
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 10 p. 2381 - 2383