乙基4-苯甲酰基苯甲酸酯合成路线 （共 21 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1-methyl-pyrrolidin-2-one T=60°C; 6 h;
参考文献
Journal of Organometallic Chemistry, , vol. 693, # 17 p. 2949 - 2953
反应条件
1: benzoyl chloride With indium; chloro-trimethyl-silane; ethylene dibromide; lithium chloride in N,N-dimethyl-formamide T=40°C; 3 h; Inert atmosphere; 2: 4-iodobenzoic acid ethyl ester With tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl-formamide T=90°C; 5 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 16, # 4 p. 1144 - 1147
反应条件
3-chloroprop-1-ene; cobalt(II) dibromide; zinc; trifluoroacetic acid in acetonitrile 20 h;
参考文献
Kazmierski, Igor; Bastienne, Mylene; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 936 - 942
反应条件
4-(N,N-dimethlyamino)pyridine; palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=90°C; 0.5 h; Microwave irradiation;
参考文献
Baburajan; Senthilkumaran; Elango, Kuppanagounder P.
New Journal of Chemistry, 2013 , vol. 37, # 10 p. 3050 - 3056
反应条件
1: 4-(ethoxycarbonyl)phenyl 4-(dimethylamino)benzenesulfonate With para-fluorostyrene; CuCN*2LiCl; phenyl-magnesium chloride; tetra-(n-butyl)ammonium iodide; cobalt(II) 2,4-pentanedionate in tetrahydrofuran; N,N'-dimethyl-N,N'-propyleneurea T=-20 - 25°C; Inert atmosphere; 2: benzoyl chloride in tetrahydrofuran; N,N'-dimethyl-N,N'-propyleneurea T=-20 - 25°C; 2.5 h; Inert atmosphere;
参考文献
Rohbogner, Christoph J.; Diene, Coura R.; Korn, Tobias J.; Knochel, Paul
Angewandte Chemie - International Edition, 2010 , vol. 49, # 10 p. 1874 - 1877
反应条件
1.1: 90 percent / TiCl4 / CH2Cl2 / 2.5 h / 20 °C 2.1: isopropylmagnesium chloride / tetrahydrofuran / -20 °C 2.2: 80 percent / iron(III) acetylacetonate / tetrahydrofuran / -10 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 22 p. 2968 - 2970
反应条件
toluene-4-sulfonic acid 2 h; Heating;
参考文献
Chen, Hua-Sin; Kuo, Sheng-Chu; Teng, Che-Ming; Lee, Fang-Yu; Wang, Jih-Pyang; Lee, Yu-Chun; Kuo, Chiung-Wen; Huang, Ching-Che; Wu, Chin-Chung; Huang, Li-Jiau
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 3 p. 1262 - 1278
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 22 p. 3746 - 3749
反应条件
copper(l) iodide; Li naphtalide; triphenylphosphine 1) THF, 0 deg C; 2) -35 deg C, 10-15 min; 3) -35 deg C, 90 min; -> r.t., 30 min; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 36 p. 4513 - 4516
