in diethyl ether
addn. of LiBH4 in ether to the hydrochloride within 20min, stirring for 3.5h, filtration after standing at 0°C for 12h;; treatment of residue with H2O;;
in tetrahydrofuran
dropwise addn. of 2.0M BH3*THF (25 mmol) to a THF soln. of the amine (10 mmol); performed under a dry N2 atm.;; not isolated, in soln. obtained;;
参考文献
Camacho, C.; Paz-Sandoval, M. A.; Contreras, R.
Polyhedron, 1986 , vol. 5, p. 1723 - 1732