2alpha-甲基环丁酮合成路线 （共 28 条）
参考文献
Ogura,K. et al.
Tetrahedron Letters, 1974 , p. 3653 - 3656
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
Girard,C. et al.
Tetrahedron Letters, 1974 , p. 3329 - 3332
反应条件
2,6-lutidine buffer in water
T=25°C; 24 h; other EtOH/water ratio; Product distribution;
参考文献
Hanack, Michael; Collins, Clair J.; Stutz, H.; Benjamin, Ben M.
Journal of the American Chemical Society, 1981 , vol. 103, # 9 p. 2356 - 2360
反应条件
sodium carbonate
T=80°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
chromium(VI) oxide in pyridine
参考文献
Julia,M. et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 260, p. 4222 - 4224
反应条件
pyridine; ozone in dichloromethane
参考文献
Conia,J.-M.; Gore,J.
Bulletin de la Societe Chimique de France, 1963 , p. 735 - 743
反应条件
sodium carbonate
T=60°C; 24 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate
T=20°C; 1 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
1: (i) B2H6, diglyme, (ii) H2O2, NaOH
2: CrO3 / pyridine
View Scheme
参考文献
Julia,M. et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 260, p. 4222 - 4224
反应条件
1: (i) HBr, (ii) (dehydrobromination)
2: (i) B2H6, diglyme, (ii) H2O2, NaOH
3: CrO3 / pyridine
View Scheme
参考文献
Julia,M. et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1965 , vol. 260, p. 4222 - 4224
