(1E)-乙烯-1,2-D2合成路线 （共 37 条）
反应条件
chloroform; bromine unter Belichtung;
参考文献
Bernstein et al.
Journal of Chemical Physics, 1952 , vol. 20, p. 1227
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Rawlings, Bernard J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 6 p. 290 - 292
反应条件
chromium dichloride
durch Reduktion mit saurer Loesung;
参考文献
Patterson; du Vigneaud
Journal of Biological Chemistry, 1938 , vol. 123, p. 331
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Douglas; Rabinovitch; Looney
Journal of Chemical Physics, 1955 , vol. 23, p. 315
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Rabinovitch; Looney
Journal of the American Chemical Society, 1953 , vol. 75, p. 2652
Org.Synth.Isotopes, 1958 , p. 1434
反应条件
in toluene
condensing ethylene oxide to Ta-complex in toluene at -196°C, stirring at room temp. for 5 d; collecting gaseous products in -78 and -115°C cold traps, IR detn.;
参考文献
Whinnery Jr., LeRoy L.; Henling, Lawrence M.; Bereaw, John E.
Journal of the American Chemical Society, 1991 , vol. 113, # 20 p. 7575 - 7582
反应条件
1: With NaOD in water-d2
2: With palladium diacetate in water-d2
T=30°C; 18 h;
参考文献
Gordillo, Alvaro; Jesus, Ernesto de; Lopez-Mardomingo, Carmen
Journal of the American Chemical Society, 2009 , vol. 131, p. 4584 - 4585
反应条件
Eu(Hg); {[Mg2Mo8O22(CH3O)6(MeOH)4](2-)[Mg(MeOH)6](2+)}*6MeOH; thiophenol in methanol
T=21°C; P=120 Torr; Further byproducts given. Title compound not separated from byproducts;
参考文献
Bardina; Bazhenova; Petrova; Shilova; Shilov
Russian Chemical Bulletin, 2006 , vol. 55, # 5 p. 793 - 801
反应条件
tetrahydrofuran; magnesium
参考文献
Schubert et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4590
反应条件
siloxene
T=190.9°C; P=28.7 Torr; 0.166667 h; other temperatures and pressures; MechanismKineticsThermodynamic data;
参考文献
Sendoda, Yoko; Ono, Yoshio
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1980 , vol. 76, p. 435 - 441
反应条件
Pd-TiO2; H2
T=150°C;
参考文献
Zhivonitko, Vladimir V.; Kovtunov, Kirill V.; Chapovsky, Pavel L.; Koptyug, Igor V.
Angewandte Chemie - International Edition, 2013 , vol. 52, # 50 p. 13251 - 13255
Angew. Chem., 2013 , vol. 125, # 50 p. 13493 - 13497,5
反应条件
apple slices in the dark, 15 deg C; Title compound not separated from byproducts;
参考文献
Adlington, Robert M.; Baldwin, Jack E.; Rawlings, Bernard J.
Journal of the Chemical Society, Chemical Communications, 1983 , # 6 p. 290 - 292
