(+)-3-甲基-2-丁醇合成路线 (共 15 条)
反应条件
4 A molecular sieve; immobilized lipase PS in di-isopropyl ether
T=30°C;
参考文献
Kato, Katsuya; Irimescu, Roxana; Saito, Takao; Yokogawa, Yoshiyuki; Takahashi, Haruo
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 1 p. 203 - 206
反应条件
immobilized lipase from Candida antarctica (Novozyme SP 435); 1-n-butyl-3-methylimidazolium bistrifluoromethylsulfonylamide
T=20°C; 61 h; atmospheric pressure;
参考文献
Reetz, Manfred T.; Wiesenhoefer, Wolfgang; Francio, Giancarlo; Leitner, Walter
Advanced Synthesis and Catalysis, 2003 , vol. 345, # 11 p. 1221 - 1228
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Seebach, Dieter; Behrendt, Linda; Felix, Dorothee
Angewandte Chemie, 1991 , vol. 103, # 8 p. 991 - 992
反应条件
3 A molecular sieve; Humicola insolens ferulic acid esterase
T=45°C; 216 h;
参考文献
Hatzakis, Nikos S.; Smonou, Ioulia
Bioorganic Chemistry, 2005 , vol. 33, # 4 p. 325 - 337
反应条件
oxonium; methyllithium
1.) ether; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Hayashi, Tamio; Kanehira, Koichi; Kumada, Makoto
Tetrahedron Letters, 1981 , vol. 22, # 44 p. 4417 - 4420