(R)-(+)-1-苯基乙醇合成路线 (共 353 条)
反应条件
methanol; [Zn4O(CF3CO2)6] 48 h; RefluxInert atmosphere;
参考文献
Iwasaki, Takanori; Agura, Kazushi; Maegawa, Yusuke; Hayashi, Yukiko; Ohshima, Takashi; Mashima, Kazushi
Chemistry - A European Journal, 2010 , vol. 16, # 38 p. 11567 - 11571
反应条件
1: Escherichia coli BioH esterase immobilized on Macroporous adsorptive resin / 35 °C / Enzymatic reaction 2: immobilized CALB lipase / di-isopropyl ether / 8 h / 35 °C / Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 22, # 9 p. 980 - 985
反应条件
sodium hydroxide in tetrahydrofuran; methanol; diethyl ether; toluene 0.5 h; Inert atmosphere;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 2 p. 314 - 320
反应条件
sodium hydroxide in tetrahydrofuran; methanol; diethyl ether; toluene 0.5 h; Inert atmosphere;
参考文献
Chemistry - An Asian Journal, , vol. 7, # 2 p. 314 - 320
反应条件
T=100 - 140°C; P=10 Torr; optical yield given as percent ee;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1877 - 1882
反应条件
(-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 13 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Journal of Organic Chemistry, , vol. 77, # 7 p. 3570 - 3575
反应条件
Lipase Amano AK T=20°C; pH=7; 30 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent ee;
参考文献
Bora, Pranjal P.; Bez, Ghanashyam; Anal, Jasha Momo H.
Journal of Molecular Catalysis B: Enzymatic, 2011 , vol. 72, # 3-4 p. 270 - 275
反应条件
lipase from candida antartica in aq. phosphate buffer T=30°C; pH=6.5; 24 h;
参考文献
Letters in Organic Chemistry, , vol. 9, # 9 p. 615 - 621
反应条件
(+)-pinanediol Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 102, # 25 p. 7590 - 7591
反应条件
sodium hydroxide; dihydrogen peroxide in tetrahydrofuran 3 h; Ambient temperature; Yield given;
参考文献
Tetrahedron Asymmetry, , vol. 2, # 7 p. 601 - 612