(R)-(+)-1-苯基乙醇合成路线 (共 353 条)
反应条件
Pseudomonas cepacia lipase; RuCl(η5-C9H7)(PPh3)2; oxygen in dichloromethane T=60°C; Esterification; dynamic kinetic resolution; 43 h; Enzymatic reaction; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Tetrahedron Letters, , vol. 40, # 34 p. 6281 - 6284
反应条件
Pseudomonas cepacia lipase; RuCl(η5-C9H7)(PPh3)2; oxygen in dichloromethane T=60°C; Esterification; dynamic kinetic resolution; 43 h; Enzymatic reaction; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Tetrahedron Letters, , vol. 40, # 34 p. 6281 - 6284
反应条件
Multistep reaction.;
参考文献
Okudomi, Masayuki; Shimojo, Megumi; Nogawa, Masaki; Hamanaka, Ayae; Taketa, Natsue; Matsumoto, Kazutsugu
Tetrahedron Letters, 2007 , vol. 48, # 48 p. 8540 - 8543
反应条件
Bacillus sp. Cohn 1872 pH=7; aq. phosphate bufferEnzymatic reaction;
参考文献
Journal of the Brazilian Chemical Society, , vol. 21, # 8 p. 1484 - 1489
反应条件
1: dihydrogen peroxide; magnesium sulfate / 14 h / 0 - 20 °C 2: Raphanus sativus L. peroxidase; 2-methoxy-phenol / 1 h / 20 °C / pH 6 / aq. phosphate buffer; Enzymatic reaction View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 23, # 8 p. 594 - 601
反应条件
CS-180 in toluene T=60°C; Kinetics;
参考文献
ChemCatChem, , vol. 5, # 1 p. 247 - 254
反应条件
Rh catalyst 23 h; var. catalysts and time, multistep reaction; Product distribution;
参考文献
Angewandte Chemie, , vol. 94, # 5 p. 369 - 370
反应条件
sodium tetrahydroborate; β-cyclodextrin in water T=20°C; 72 h; the regio- and enantioselective reduction of substituted styrenic epoxides; Product distribution;
参考文献
Bulletin de la Societe Chimique de France, , vol. 133, # 2 p. 161 - 166
反应条件
lipase Amano PS enzyme in di-isopropyl ether T=30°C; 11 h; other enzyme, varying reaction time; Product distribution;
参考文献
Tetrahedron Letters, , vol. 37, # 41 p. 7369 - 7372
反应条件
aluminium trichloride in toluene T=-5°C; 17 h; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 16 p. 1713 - 1719