反式-alpha-甲基肉桂醛合成路线 （共 62 条）
反应条件
potassium hydroxide; nBu4NPF6 in benzene T=20°C; 4 h;
参考文献
Kryshtal, Galina V.; Zhdankina, Galina M.; Zlotin, Sergei G.
European Journal of Organic Chemistry, 2005 , # 13 p. 2822 - 2827
反应条件
pyridine; air; Pd(II)-hydrotalcite in toluene T=65°C; P=760.051 Torr; 15 h;
参考文献
Kakiuchi; Maeda; Nishimura; Uemura
Journal of Organic Chemistry, 2001 , vol. 66, # 20 p. 6620 - 6625
反应条件
[(P{(C6H11)3})2Pd(Cl)2]; hydrogen; triethylamine in benzene T=155°C; P=53200 Torr; 6 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ishii; Miyashita; Kamita; Hidai
Journal of the American Chemical Society, 1997 , vol. 119, # 27 p. 6448 - 6449
反应条件
sodium carbonate; [Cp*IrCl2]2 in 1,3,5-trimethyl-benzene T=100 - 140°C; 18 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 16 p. 6285 - 6286
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-78°C; 12 h;
参考文献
Concellon, Jose M.; Rodriguez-Solla, Humberto; Del Amo, Vicente; Diaz, Pamela
Synthesis, 2009 , # 15 art. no. Z09909SS, p. 2634 - 2645
反应条件
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium dichloride in 1,2-dichloro-ethane T=50°C; 2 h; stereoselective reaction;
参考文献
Chen, Huoji; Jiang, Huanfeng; Cai, Congbi; Dong, Jia; Fu, Wei
Organic Letters, 2011 , vol. 13, # 5 p. 992 - 994
反应条件
oxygen; sodium acetate; acetylacetone; palladium diacetate in propionic acid T=90°C; P=760.051 Torr; 1.5 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 14 p. 5471 - 5474
反应条件
[(P{(C6H11)3})2Pd(Cl)2]; hydrogen; triethylamine in benzene T=155°C; P=53200 Torr; 6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 119, # 27 p. 6448 - 6449
反应条件
1: With zinc dibromide in tetrahydrofuran T=20°C; 5 h; 2: With water in tetrahydrofuran T=20°C; 1 h;
参考文献
Lahmar, Nour; Aatar, Jamaa; Ayed, Taicir Ben; Amri, Hassen; Bellassoued, Moncef
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 3018 - 3026
反应条件
hydrogenchloride in diethyl ether T=20°C; 0.5 h;
参考文献
Tay, M. K.; Aboujaoude, E. E.; Collignon, N.; Savignac, Ph.
Tetrahedron Letters, 1987 , vol. 28, # 12 p. 1263 - 1266
