反式-alpha-甲基肉桂醛合成路线 （共 62 条）
反应条件
1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 3 h / -78 °C 2: manganese(IV) oxide / hexane / 20 h / 20 °C View Scheme
参考文献
Chemical Communications, , vol. 50, # 31 p. 4119 - 4122
反应条件
zinc(II) chloride; zinc dibromide 1) THF, RT, 2 h, 2) ether, water, 18 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 58, # 9 p. 2517 - 2522
反应条件
titanium tetrachloride
参考文献
Tetrahedron Letters, , vol. 23, # 32 p. 3257 - 3260
反应条件
sec.-butyllithium; trifluoroacetic acid 1.) THF, cyclohexane, -78 deg C, 0.5 h, -20 deg C, 1 h; 2.) 0 deg C, 13 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 29, # 32 p. 3895 - 3898
反应条件
sec.-butyllithium; oxalic acid 1.) THF, cyclohexane, -78 deg C, 0.5 h, -20 deg C, 1 h; 2.) 0 deg C, 13 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 29, # 32 p. 3895 - 3898
反应条件
zinc dibromide in tetrahydrofuran T=20°C; 24 h; Product distribution; Further Variations:CatalystsSolventsTemperatures;
参考文献
Lahmar, Nour; Aatar, Jamaa; Ayed, Taicir Ben; Amri, Hassen; Bellassoued, Moncef
Journal of Organometallic Chemistry, 2006 , vol. 691, # 13 p. 3018 - 3026
反应条件
Multistep reaction.;
参考文献
Tetrahedron Letters, , vol. 49, # 3 p. 543 - 547
反应条件
(i) TiCl4, CH2Cl2, (ii) H2O; Multistep reaction;
参考文献
Chemistry Letters, , p. 859 - 862
反应条件
multistep reaction, var. aldehydes.; Product distribution;
参考文献
Tay, M. K.; Aboujaoude, E. E.; Collignon, N.; Savignac, Ph.
Tetrahedron Letters, 1987 , vol. 28, # 12 p. 1263 - 1266
反应条件
Yield given. Multistep reaction;
参考文献
Angewandte Chemie, , vol. 92, # 10 p. 841 - 842
