反式-alpha-甲基肉桂醛合成路线 (共 62 条)
反应条件
(η5-C5Ph5)Ru(CO)2Cl; potassium tert-butylate; sodium carbonate in tetrahydrofuran; toluene T=35°C; 13 h; Inert atmosphere;
参考文献
Bartoszewicz, Agnieszka; Jezowska, Martina M.; Laymand, Kevin; Moebus, Juri; Martin-Matute, Belen
European Journal of Inorganic Chemistry, 2012 , # 9 p. 1517 - 1530
反应条件
1: With 3-methyl-2-amino-pyridine; Wilkinson's catalyst; α,α,α-Trifluoro-p-toluic acid; cyclohexylamine in toluene T=130°C; 12 h; 2: With hydrogenchloride; water in tetrahydrofuran
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 1926 - 1930
反应条件
T=470.2°C; P=103.2 - 203 Torr; Kinetics; Further Variations:PressuresTemperaturesReagentssurface-to-volume ratio;
参考文献
Chaban, Omar Y.; Dominguez, Rosa M.; Herize, Armando; Tosta, Maria; Cuenca, Angela; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 2007 , vol. 20, # 5 p. 307 - 312
反应条件
1: With 3-methyl-2-amino-pyridine; Wilkinson's catalyst; α,α,α-Trifluoro-p-toluic acid; cyclohexylamine in toluene T=130°C; 12 h; 2: With hydrogenchloride; water in tetrahydrofuran
参考文献
Cha, Kyung-Mi; Lee, Hyejeong; Park, Jung-Woo; Lee, Yura; Jo, Eun-Ae; Jun, Chul-Ho
Chemistry - An Asian Journal, 2011 , vol. 6, # 8 p. 1926 - 1930
反应条件
palladium diacetate in cyclohexane T=140°C; 24 h; Molecular sieveair;
参考文献
Chemical Communications, , vol. 48, # 35 p. 4253 - 4255
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; air; triphenylphosphine in 1,4-dioxane 24 h; Heating;
参考文献
Iwai, Tomohiro; Fujihara, Tetsuaki; Tsuji, Yasushi
Chemical Communications, 2008 , # 46 p. 6215 - 6217
反应条件
T=470.2°C; P=103.2 - 203 Torr; Kinetics; Further Variations:PressuresTemperaturesReagentssurface-to-volume ratio;
参考文献
Chaban, Omar Y.; Dominguez, Rosa M.; Herize, Armando; Tosta, Maria; Cuenca, Angela; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 2007 , vol. 20, # 5 p. 307 - 312
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; air; triphenylphosphine in 1,4-dioxane 24 h; Heating;
参考文献
Iwai, Tomohiro; Fujihara, Tetsuaki; Tsuji, Yasushi
Chemical Communications, 2008 , # 46 p. 6215 - 6217
反应条件
T=470.2°C; P=103.2 - 203 Torr; Kinetics; Further Variations:PressuresTemperaturesReagentssurface-to-volume ratio;
参考文献
Chaban, Omar Y.; Dominguez, Rosa M.; Herize, Armando; Tosta, Maria; Cuenca, Angela; Chuchani, Gabriel
Journal of Physical Organic Chemistry, 2007 , vol. 20, # 5 p. 307 - 312
反应条件
1: 85 percent / 30 percent H2O2 / bis(2-nitrophenyl) diselenide / CH2Cl2 / 128 h / Ambient temperature; further. reag. and cat.; var. time 2: 88 percent / cc. HCl / tetrahydrofuran; H2O / 7 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 43, # 12 p. 2853 - 2872