反式-alpha-甲基肉桂醛合成路线 (共 62 条)
反应条件
1: With 3-methyl-2-amino-pyridine; Wilkinson's catalyst; α,α,α-Trifluoro-p-toluic acid; cyclohexylamine in toluene T=130°C; 12 h; 2: With hydrogenchloride; water in tetrahydrofuran
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 1926 - 1930
反应条件
1: With 3-methyl-2-amino-pyridine; Wilkinson's catalyst; α,α,α-Trifluoro-p-toluic acid; cyclohexylamine in toluene T=130°C; 12 h; 2: With hydrogenchloride; water in tetrahydrofuran
参考文献
Chemistry - An Asian Journal, , vol. 6, # 8 p. 1926 - 1930
反应条件
in tetrahydrofuran T=20°C; 8 h; Product distribution; Further Variations:reaction times;
参考文献
Nudelman; Garcia
Journal of Organic Chemistry, 2001 , vol. 66, # 4 p. 1387 - 1394
反应条件
sodium tetrahydroborate in ethanol
参考文献
TAKASAGO INTERNATIONAL CORPORATION
Patent: US2011/201819 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
dicobalt octacarbonyl; water in ethylene glycol dimethyl ether 2 h; Heating;
参考文献
Tetrahedron Letters, , vol. 44, # 14 p. 2775 - 2778
反应条件
potassium dihydrogenphosphate; (NH4)HPO4; magnesium sulfate in water T=28 - 32°C; 4 h; commercial baker's yeast, sugar beet molasses; Title compound not separated from byproducts;
参考文献
Fronza, Giovanni; Fuganti, Claudio; Grasselli, Piero; Majori, Luisella; Pedrocchi-Fantoni, Giuseppe; Spreafico, Franca
Journal of Organic Chemistry, 1982 , vol. 47, # 17 p. 3289 - 3296
反应条件
4-(N,N-dimethlyamino)pyridine; formic acid; Rh6(CO)12; carbon monoxide in tetrahydrofuran T=30°C; P=3800 Torr; 10 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 7 p. 2378 - 2381
反应条件
baker's yeast; D-glucose; resin XAD 1180 in water T=28°C; 24 h;
参考文献
Tetrahedron, , vol. 54, # 49 p. 15017 - 15026
反应条件
baker's yeast; D-glucose in water T=28°C; 24 h;
参考文献
Tetrahedron, , vol. 54, # 49 p. 15017 - 15026
反应条件
D-glucose; water T=20°C; 24 h; baker's yeast; Yields of byproduct given;
参考文献
Sunjic, Vitomir; Majeric, Maja; Hamersak, Zdenko
Croatica Chemica Acta, 1996 , vol. 69, # 2 p. 643 - 660