4-甲氧基-N,N-二甲基-苯甲胺合成路线 （共 38 条）
反应条件
in diethyl ether; water
T=20°C;
参考文献
Tayama, Eiji; Kimura, Hiroshi
Angewandte Chemie - International Edition, 2007 , vol. 46, # 46 p. 8869 - 8871
反应条件
1: With titanium(IV) isopropylate; triethylamine in ethanol
T=25°C; 12 h;
2: With sodium tetrahydroborate in ethanol
T=25°C; 12 h;
参考文献
Feng, Ruokun; Yao, Jinzhong; Liang, Zunjun; Liu, Zhanxiang; Zhang, Yuhong
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3688 - 3696
反应条件
NiCuFeO(x) in anhydrous xylene
24 h; Inert atmosphereSealed tubeReflux;
参考文献
Cui, Xinjiang; Dai, Xingchao; Deng, Youquan; Shi, Feng
Chemistry - A European Journal, 2013 , vol. 19, # 11 p. 3665 - 3675
反应条件
methyltrichloromonosilane in acetonitrile
T=0°C; 68 h;
参考文献
Cooper, Mark S.; Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1989 , vol. 45, # 4 p. 1155 - 1166
反应条件
chloro-trimethyl-silane in acetonitrile
T=0°C; 24 h;
参考文献
Cooper, Mark S.; Fairhurst, Robin A.; Heaney, Harry; Papageorgiou, George; Wilkins, Robert F.
Tetrahedron, 1989 , vol. 45, # 4 p. 1155 - 1166
反应条件
hydrogen in hexane
T=160°C; 48 h; Autoclave;
参考文献
Cui, Xinjiang; Dai, Xingchao; Zhang, Yan; Deng, Youquan; Shi, Feng
Chemical Science, 2014 , vol. 5, # 2 p. 649 - 655
反应条件
1: 72 percent / triethylamine / diethyl ether
2: 88 percent / polymethylhydrosiloxane / chloroplatinic acid hexahydrate / tetrahydrofuran / 3 h / 60 °C
View Scheme
参考文献
Hanada, Shiori; Motoyama, Yukihiro; Nagashima, Hideo
Tetrahedron Letters, 2006 , vol. 47, # 35 p. 6173 - 6177
反应条件
hydrogen in hexane
T=170°C; 48 h;
参考文献
Cui, Xinjiang; Dai, Xingchao; Zhang, Yan; Deng, Youquan; Shi, Feng
Chemical Science, 2014 , vol. 5, # 2 p. 649 - 655
反应条件
in dichloromethane
72 h; Ambient temperature;
参考文献
Cooper, Mark S.; Heaney Harry
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5011 - 5014
反应条件
in dichloromethane
21 h; Ambient temperature;
参考文献
Cooper, Mark S.; Heaney Harry
Tetrahedron Letters, 1986 , vol. 27, # 41 p. 5011 - 5014
