4-甲氧基-N,N-二甲基-苯甲胺合成路线 (共 38 条)
参考文献
Sharma; Talwar; Gupta, Anu; Kishore, Lalit
Journal of the Indian Chemical Society, 1997 , vol. 74, # 3 p. 233 - 234
反应条件
NaY faujasite
T=90°C; 22 h;
参考文献
Selva, Maurizio; Tundo, Pietro
Tetrahedron Letters, 2003 , vol. 44, # 44 p. 8139 - 8142
反应条件
1: sodium hydrogensulfite / ethanol / 16 h / 30 - 35 °C
2: sodium cyanoborohydride / methanol / 20 h / 20 °C
View Scheme
参考文献
Barniol-Xicota, Marta; Turcu, Andreea L.; Codony, Sandra; Escolano, Carmen; Vazquez, Santiago
Tetrahedron Letters, 2014 , vol. 55, # 15 p. 2548 - 2550
反应条件
reductive N,N-dimethylation;
参考文献
Gilday, John, P.; Negri, Joanna T.; Widdowson, David A.
Tetrahedron, 1989 , vol. 45, # 14 p. 4605 - 4618
反应条件
in chloroform; acetic acid
Kinetics; mixing the dimer cyclopalladated complex in CHCl3 and 2-phenylpyridine in HOAc with glacial acetic acid, thermostating (75°C); not isolated; spectrophotometrical detn.;
参考文献
Ryabov, Alexander D.
Inorganic Chemistry, 1987 , vol. 26, p. 1252 - 1260
参考文献
Stedman
Journal of the Chemical Society, 1927 , p. 1904
参考文献
Eliel et al.
Journal of Organic Chemistry, 1954 , vol. 19, p. 1693,1695
参考文献
Stevens
Journal of the Chemical Society, 1930 , p. 2107,2112
反应条件
T=40°C; bei der elektrolytischen Reduktion, hohe Stromdichte;
参考文献
Kindler
Archiv der Pharmazie (Weinheim, Germany), 1927 , p. 390,400
Chem. Zentralbl., 1924 , vol. 95, # II p. 1404
反应条件
1: 1.) n-butyllithium / 1.) ether, r.t., 24 h, 2.) 2 h
3: 79 percent / ethanol / 24 h / Ambient temperature
4: 1.) PCl5, 2.) NaBH4 / 1.) CHCl3, r.t., 4 h, 2.) CH3OH, r.t., 24 h
View Scheme
参考文献
Mali, R. S.; Patil, S. L.; Rodricks, Nandini R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 256 - 258