7,7,8,8-四氰基对苯二醌二甲烷合成路线 (共 50 条)
反应条件
in acetonitrile Heating;
参考文献
Odom, Susan A.; Caruso, Mary M.; Finke, Aaron D.; Prokup, Alex M.; Ritchey, Joshua A.; Leonard, John H.; White, Scott R.; Sottos, Nancy R.; Moore, Jeffrey S.
Advanced Functional Materials, 2010 , vol. 20, # 11 p. 1721 - 1727
反应条件
in acetonitrile T=200°C; sealed tube;
参考文献
Tetrahedron Letters, , vol. 27, # 30 p. 3475 - 3478
反应条件
in acetonitrile T=200°C; sealed tube;
参考文献
Tetrahedron Letters, , vol. 27, # 30 p. 3475 - 3478
反应条件
0.0833333 h; Heating;
参考文献
Bespalov, B. P.; Getmanova, E. V.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 2017 - 2020
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 11 p. 2358 - 2362
反应条件
hydrogenchloride in toluene inert atmosphere; addn. of org. compd. soln. to soln. of Ge-compd. at room temp., soln. decantation after 12 h, ppt. hydrolysis (HCl); soln. filtration for obtaining Ph3GeGePh3, extn. (ether), drying (Na2SO4), soln. concn. (reduced pressure); (1)H NMR;
参考文献
Riviere, P.; Castel, A.; Desor, D.; Abdennadher, C.
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 51 - 60
反应条件
hydrogenchloride in toluene inert atmosphere; addn. of org. compd. soln. to soln. of Ge-compd. at room temp., soln. decantation after 12 h, ppt. hydrolysis (HCl); soln. filtration for obtaining Ph3GeGePh3, extn. (ether), drying (Na2SO4), soln. concn. (reduced pressure); (1)H NMR;
参考文献
Riviere, P.; Castel, A.; Desor, D.; Abdennadher, C.
Journal of Organometallic Chemistry, 1993 , vol. 443, # 1 p. 51 - 60
反应条件
in dimethyl sulfoxide; acetonitrile T=11°C; Equilibrium constantRate constant;
参考文献
Kampar, V. E.; Tsiekure, V. P.; Kreitsberga, Ya. N.; Neiland, O. Ya.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 8 p. 1870 - 1874,1605 - 1608
反应条件
hydrogenchloride in toluene inert atmosphere; addn. of org. compd. soln. to soln. of Ge-compd. at room temp., soln. decantation after 12 h, ppt. hydrolysis (HCl); soln. filtration for obtaining Ph3GeGePh3, extn. (ether), drying (Na2SO4), soln. concn. (reduced pressure); (1)H NMR;
参考文献
Journal of Organometallic Chemistry, , vol. 443, # 1 p. 51 - 60
反应条件
0.0833333 h; Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 16, p. 2017 - 2020
Zhurnal Organicheskoi Khimii, , vol. 16, # 11 p. 2358 - 2362
反应条件
in dimethyl sulfoxide; acetonitrile T=11°C; Equilibrium constantRate constant;
参考文献
Kampar, V. E.; Tsiekure, V. P.; Kreitsberga, Ya. N.; Neiland, O. Ya.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 8 p. 1870 - 1874,1605 - 1608