(R)-(+)-2,2-二甲基-1,3-二氧戊环-4-甲醛合成路线 (共 94 条)
反应条件
lead(IV) acetate in ethyl acetate 3 h;
参考文献
Journal of Organic Chemistry, , vol. 60, # 16 p. 5236 - 5242
反应条件
oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-78 - 20°C; Swern oxidation; Inert atmosphere;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 49, # 2 p. 260 - 263
反应条件
sodium periodate; sodium hydrogencarbonate in dichloromethane
参考文献
Tetrahedron, , vol. 66, # 6 p. 1267 - 1273
反应条件
1: With zinc(II) chloride 2: With sodium periodate in dichloromethane
参考文献
Journal of Organic Chemistry, , vol. 75, # 1 p. 74 - 85
反应条件
sodium periodate in tetrahydrofuran; water 1 h;
参考文献
Tetrahedron, , vol. 41, # 15 p. 3117 - 3126
反应条件
ozone; triphenylphosphine in dichloromethane
参考文献
Tetrahedron Letters, , vol. 27, # 23 p. 2575 - 2578
反应条件
diisobutylaluminium hydride in tetrahydrofuran; dichloromethane T=-78°C; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 59, # 5 p. 1210 - 1212
反应条件
lead(IV) acetate; sodium carbonate in dichloromethane 0.166667 h;
参考文献
Helvetica Chimica Acta, , vol. 66, # 3 p. 814 - 823
反应条件
sodium periodate; sodium hydrogencarbonate T=10 - 15°C; 6 h;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 107, # 6 p. 455 - 458
反应条件
sodium periodate; sodium hydrogencarbonate in dichloromethane; water T=0 - 20°C; 0.75 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 352, # 18 p. 3329 - 3338