2-(叔丁氧基羰基)-3-氧代-3-苯基丙酸乙酯合成路线 （共 5 条）
反应条件
n-butyllithium in tetrahydrofuran; hexane T=-80 - -50°C; 2 h;
参考文献
Schmidt; Griesser; Lieberknecht; Grather
Synthesis, 1993 , # 8 p. 765 - 766
反应条件
dirhodium(II) tetraoctanoate in dichloromethane
参考文献
Bourdon, Lisa H.; Fairfax, David J.; Martin, Gregory S.; Mathison, Casey J.; Zhichkin, Pavel
Tetrahedron Asymmetry, 2004 , vol. 15, # 22 p. 3485 - 3487
反应条件
1: DMAP / acetonitrile / 18 h / Ambient temperature 2: 91 percent / LDA, DMPU / hexane; tetrahydrofuran / 1 h / -78 °C View Scheme
参考文献
Schmidt; Griesser; Lieberknecht; Grather
Synthesis, 1993 , # 8 p. 765 - 766
反应条件
1: 2 M aq. KHCO3 / dioxane / Ambient temperature 2: 10.8 g / 1 M aq. NaOH / dioxane / Ambient temperature 3: 85 percent / 1.6 M BuLi / tetrahydrofuran; hexane / 2 h / -80 - -50 °C View Scheme
参考文献
Schmidt; Griesser; Lieberknecht; Grather
Synthesis, 1993 , # 8 p. 765 - 766
反应条件
1: 10.8 g / 1 M aq. NaOH / dioxane / Ambient temperature 2: 85 percent / 1.6 M BuLi / tetrahydrofuran; hexane / 2 h / -80 - -50 °C View Scheme
参考文献
Schmidt; Griesser; Lieberknecht; Grather
Synthesis, 1993 , # 8 p. 765 - 766
