(R)-(+)-甲基对甲苯亚砜合成路线 (共 72 条)
反应条件
in diethyl ether; benzene T=0 - 20°C;
参考文献
Bode, Moira L.; Gates, Paul J.; Gebretnsae, Samson Y.; Vleggaar, Robert
Tetrahedron, 2010 , vol. 66, # 11 p. 2026 - 2036
反应条件
C88H90N2O6P2; dihydrogen peroxide; magnesium sulfate in cyclohexane; water T=20°C; 2 h; optical yield given as percent eeenantioselective reaction;
参考文献
Liao, Saihu; Coric, Ilija; Wang, Qinggang; List, Benjamin
Journal of the American Chemical Society, 2012 , vol. 134, # 26 p. 10765 - 10768
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 639 - 640
反应条件
methylmagnesium bromide in toluene T=-40°C; 3 h;
参考文献
Shibata, Norio; Matsunaga, Mitsuharu; Nakagawa, Masaya; Fukuzumi, Takeo; Nakamura, Shuichi; Toru, Takeshi
Journal of the American Chemical Society, 2005 , vol. 127, # 5 p. 1374 - 1375
反应条件
camphorlactone-sulfonyloxaziridine in tetrachloromethane 70 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Davis, Franklin A.; Weismiller, Michael C.; Murphy, Christopher K.; Reddy, R. Thimma; Chen, Band-Chi
Journal of Organic Chemistry, 1992 , vol. 57, # 28 p. 7274 - 7285
反应条件
in tetrahydrofuran; diethyl ether T=-30°C; 0.416667 h;
参考文献
Corey; Weigel; Chamberlin; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 21 p. 6613 - 6615
参考文献
Liera, Jose M.; Fernandez, Inmaculada; Alcudia, Felipe
Tetrahedron Letters, 1991 , vol. 32, # 49 p. 7299 - 7302
反应条件
titanium(IV) isopropylate; alpha,alpha-dimethylbenzyl hydroperoxide; C22H30O12 in dichloromethane; water T=-20°C; 1 h; Inert atmosphere; Kinetics; Reagent/catalystConcentrationTimeSolvent; enantioselective reaction;
参考文献
Newhouse, Timothy R.; Li, Xin; Blewett, Megan M.; Whitehead, Clare M. C.; Corey
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17354 - 17357
反应条件
C78H105N3O3*3H(1+)*O40PW12(3-); dihydrogen peroxide in chloroform; water; acetonitrile T=35°C; 0.0833333 h; optical yield given as percent eeenantioselective reaction;
参考文献
Jahier, Claire; Coustou, Marie-Flora; Cantuel, Martine; McClenaghan, Nathan D.; Buffeteau, Thierry; Cavagnat, Dominique; Carraro, Mauro; Nlate, Sylvain
European Journal of Inorganic Chemistry, 2011 , # 5 p. 727 - 738
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 69, # 23 p. 8070 - 8076