(R)-(+)-甲基对甲苯亚砜合成路线 （共 72 条）
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 69, # 23 p. 8070 - 8076
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 69, # 23 p. 8070 - 8076
反应条件
1: methyl iodide With magnesium in diethyl ether T=20°C; 2 h; 2: (1R,2S,5R,SS)-(-)-menthyl p-toluenesulfinate in diethyl ether; toluene T=0 - 20°C; 3 h;
参考文献
Rival, Nicolas; Hazelard, Damien; Hanquet, Gilles; Kreuzer, Thomas; Bensoussan, Charlelie; Reymond, Sebastien; Cossy, Janine; Colobert, Francoise
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 47 p. 9418 - 9428
反应条件
in toluene T=-60 - -20°C;
参考文献
Satoh, Tsuyoshi; Oohara, Teruhiko; Ueda, Yoshiko; Yamakawa, Koji
Journal of Organic Chemistry, 1989 , vol. 54, # 13 p. 3130 - 3136
反应条件
(DHQD)2Pyr; dihydrogen peroxide; WO3 in tetrahydrofuran T=25°C; 16 h; Title compound not separated from byproducts;
参考文献
Thakur, Vinay V.; Sudalai
Tetrahedron Asymmetry, 2003 , vol. 14, # 4 p. 407 - 410
反应条件
1: in tetrahydrofuran T=-78 - 22°C; 0.5 h; 2: With water; potassium hydrogencarbonate in tetrahydrofuran
参考文献
APSINTERM LLC
Patent: JP2005/522525 A, 2005 ;
Location in patent: Page/Page column 59-60 ;
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; Substitution; 0.5 h;
参考文献
Journal of Organic Chemistry, , vol. 64, # 20 p. 7559 - 7567
反应条件
in tetrahydrofuran T=-78°C; 1 h;
参考文献
Oppolzer, Wolfgang; Froelich, Olivier; Wiaux-Zamar, Chantal; Bernardinelli, Gerald
Tetrahedron Letters, 1997 , vol. 38, # 16 p. 2825 - 2828
反应条件
tin(ll) chloride in acetonitrile T=25°C; Irradiation;
参考文献
Organic Letters, , vol. 13, # 1 p. 142 - 145
反应条件
in tetrahydrofuran; diethyl ether T=-78°C; Substitution;
参考文献
Davis, Franklin A.; Liu, Hu; Zhou, Ping; Fang, Tianan; Reddy, G. Venkat; Zhang, Yulian
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7559 - 7567
