2,5-二己氧基对苯二甲醛合成路线 (共 3 条)
反应条件
1: 1,4-dibromo-2,5-bis(hexyloxy)-benzene With n-butyllithium in diethyl ether; hexane 1 h; Heating; 2: N,N-dimethyl-formamide T=0 - 20°C;
参考文献
Sarker, Ananda M.; Ding, Liming; Lahti, Paul M.; Karasz, Frank E.
Macromolecules, 2002 , vol. 35, # 1 p. 223 - 230
反应条件
1: 1,4-dibromo-2,5-bis(hexyloxy)-benzene With n-butyllithium in diethyl ether; n-heptane T=-20 - 20°C; 2: N,N-dimethyl-formamide in diethyl ether T=20°C; Bouveault reaction; 1 h; Further stages.;
参考文献
Meier, Herbert; Lehmann, Matthias; Holst, Hans Christof; Schwoeppe, Dirk
Tetrahedron, 2004 , vol. 60, # 32 p. 6881 - 6888
反应条件
n-butyllithium in diethyl ether; hexane 1.) 0 deg C, 2.) room temperature, 2 h;
参考文献
Peng, Zhonghua; Gharavi, Ali R.; Yu, Luping
Journal of the American Chemical Society, 1997 , vol. 119, # 20 p. 4622 - 4632