(E,E,E)-S2,4,6-辛三烯合成路线 (共 22 条)
反应条件
potassium tert-butylate in dimethyl sulfoxide
参考文献
van Dongen,J.P.C.M. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1967 , vol. 86, p. 1077 - 1081
反应条件
1: diethyl ether / -15 - 5 °C 2: p-toluene-sulfonic acid / 11 Torr / beim Destillieren View Scheme
参考文献
Doering,W. von E.; Beasley,G.H.
Tetrahedron, 1973 , vol. 29, p. 2231 - 2243
反应条件
C56H77N2OW T=20°C; 16 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Townsend, Erik M.; Schrock, Richard R.; Hoveyda, Amir H.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11334 - 11337
反应条件
bis(1,5-cyclooctadiene)nickel (0); CH3NHCH(CH3)CH(Ph)OPPh2 in toluene T=40°C; 0.333333 h; other catalysts, other times; Product distribution;
参考文献
Denis, Philippe; Mortreux, Andre; Petit, Francis; Buono, Gerard; Peiffer, Gilbert
Journal of Organic Chemistry, 1984 , vol. 49, # 26 p. 5274 - 5276
参考文献
Albriktsen,P.; Harris,R.K.
Acta Chemica Scandinavica (1947-1973), 1973 , vol. 27, p. 1875 - 1882
反应条件
L-ISOLEUCIPHOS; bis(1,5-cyclooctadiene)nickel (0) in methanol; toluene T=60°C; 6 h; other cocatalysts (ligands), other temperatures, other reaction times, other proportions of ligands, solvent, and reactants; Product distribution;
参考文献
Masotti, Henriette; Pfeiffer, Gilbert; Siv, Chhan; Courbis, Pierre; Sergent, Michelle; Phan TAN LUU, Roger
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 1 p. 63 - 77
反应条件
zirconium tetra-n-butoxide; diethylaluminium chloride; triphenylphosphine in toluene T=100°C; 8 h; Product distribution;
参考文献
Dzhemilev, U. B.; Ibragimov, A. G.; Tolstikov, G. A.; Vostrikova, O. S.; Zelenova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2313 - 2319
反应条件
zirconium tetra-n-butoxide; diethylaluminium chloride; triphenylphosphine in toluene T=100°C; 8 h; Product distribution;
参考文献
Dzhemilev, U. B.; Ibragimov, A. G.; Tolstikov, G. A.; Vostrikova, O. S.; Zelenova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2313 - 2319
反应条件
T=240 - 260°C; unter vermindertem Druck;
参考文献
Woods; Viola
Journal of the American Chemical Society, 1956 , vol. 78, p. 4380,4382
Full Text Show Details
Alder; v. Brachel
Justus Liebigs Annalen der Chemie, 1957 , vol. 608, p. 195,198
反应条件
zirconium tetra-n-butoxide; diethylaluminium chloride; triphenylphosphine in toluene T=100°C; 8 h; Product distribution;
参考文献
Dzhemilev, U. B.; Ibragimov, A. G.; Tolstikov, G. A.; Vostrikova, O. S.; Zelenova, L. M.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2066 - 2071
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2313 - 2319