4-叔丁基苯并-15-冠-5合成路线 (共 4 条)
参考文献
Tashmukhamedova, A. K.; Stempnevskaya, I. A.; Saifullina, N. Zh.; Levkovich, M. G.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 11 p. 1178 - 1185
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 11 p. 1461 - 1469
反应条件
sodium hydroxide in butan-1-ol 30 h; Heating;
参考文献
Beger, J.; Meerbote, M.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 1 p. 2 - 9
反应条件
1: 69 percent / Wofatit OK 80 / xylene / 140 - 145 °C 2: 62 percent / NaOH / butan-1-ol / 30 h / Heating View Scheme
参考文献
Beger, J.; Meerbote, M.
Journal fuer Praktische Chemie (Leipzig), 1985 , vol. 327, # 1 p. 2 - 9
反应条件
1: 3,4-dihydroxy-1-tert-butylbenzene With caesium carbonate in acetonitrile 3 h; RefluxInert atmosphere; 2: pentaethylene glycol bis(methanesulfonate) in acetonitrile Inert atmosphereReflux;
参考文献
Hanes, Robert E.; Lee, Jong Chan; Ivy, Sheryl N.; Palka, Anna; Bartsch, Richard A.
Arkivoc, 2010 , vol. 2010, # 7 p. 238 - 248