O,O,S-三甲基硫代磷酸酯合成路线 （共 37 条）
反应条件
1: dithiophosphorus acid O,O-dimethyl ester With chlorine in toluene T=5 - 10°C; 1.5 h; Heating / reflux; 2: With potassium hydroxide in water; toluene pH=> 7.0; 3: methyl iodide in acetonitrile T=20°C; 10 h;
参考文献
US2007/10496 A1, ;
Page/Page column 12 ;
反应条件
2,4,6-trichloro-1,3,5-triazine in acetonitrile T=80°C; 1 h;
参考文献
Liu, Tianzhen; Cui, Xiaoxue; Yu, Zhifang; Li, Chunbao
Phosphorus, Sulfur and Silicon and the Related Elements, 2012 , vol. 187, # 5 p. 606 - 611
反应条件
in dichloromethane 0.5 h;
参考文献
Poulter, C. Dale; Mautz, Douglas S.
Journal of the American Chemical Society, 1991 , vol. 113, # 13 p. 4895 - 4903
反应条件
boron trifluoride-methanol 1) 0 deg C, 1h, 2) RT, overnight;
参考文献
Ryu, Seungmin; Jackson, John A.; Thompson, Charles M.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 4999 - 5002
反应条件
MPPA; magnesium salt in dichloromethane 12 h; Heating;
参考文献
Jackson; Berkman; Thompson
Tetrahedron Letters, 1992 , vol. 33, # 41 p. 6061 - 6064
反应条件
boron trifluoride-methanol 1) 0 deg C, 1h, 2) RT, overnight;
参考文献
Ryu, Seungmin; Jackson, John A.; Thompson, Charles M.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 4999 - 5002
反应条件
boron trifluoride-methanol 1) 0 deg C, 1h, 2) RT, overnight;
参考文献
Ryu, Seungmin; Jackson, John A.; Thompson, Charles M.
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 4999 - 5002
参考文献
Journal of the Chemical Society, , vol. 99, p. 719
反应条件
boron trifluoride diethyl etherate in dichloromethane
参考文献
Tetrahedron Letters, , vol. 38, # 10 p. 1859 - 1862
反应条件
oxygen in acetone 0.0333333 h; Plasma treatment;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 57, # 14 p. 6238 - 6245
