1-(对羟基苯基)-2-硫脲合成路线 (共 15 条)
反应条件
sodium hydroxide T=75 - 80°C; 0.333333 h;
参考文献
Rasmussen, C. R.; Villani, F. J.; Weaner, L. E.; Reynolds, B. E.; Hood, A. R.; et al.
Synthesis, 1988 , # 6 p. 456 - 459
反应条件
1: Ammonium thiocyanate With benzoyl chloride in acetone 3 h; Inert atmosphereReflux; 2: 4-amino-phenol in acetone 1 h; Inert atmosphereReflux;
参考文献
Achenbach, Janosch; Klingler, Franca-Maria; Bloecher, Rene; Moser, Daniel; Haefner, Ann-Kathrin; Roedl, Carmen B.; Kretschmer, Simon; Krueger, Bjoern; Loehr, Frank; Stark, Holger; Hofmann, Bettina; Steinhilber, Dieter; Proschak, Ewgenij
ACS Medicinal Chemistry Letters, 2013 , vol. 4, # 12 p. 1169 - 1172
反应条件
ethanol; ammonia; water
参考文献
Journal of the Chemical Society, , vol. 125, p. 1704
反应条件
[bis(acetoxy)iodo]benzene; ammonia in water; acetonitrile 0.5 h; Cooling with ice;
参考文献
Tetrahedron Letters, , vol. 50, # 20 p. 2407 - 2410
参考文献
Willson, M; Perie, JJ; Malecaze, F; Opperdoes, F; Callens, M
European Journal of Medicinal Chemistry, 1992 , vol. 27, # 8 p. 799 - 808
反应条件
1: acetone / Ambient temperature 2: 2.0 N aq. NaOH / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 40, # 12 p. 1901 - 1905
反应条件
1: in acetone T=20°C; 3 h; 2: With sodium hydroxide in tetrahydrofuran; acetone T=20°C; 4 h;
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 1 p. 111 - 114
参考文献
Chemische Berichte, , vol. 16, p. 1828
反应条件
2: ammonia View Scheme
参考文献
Chemische Berichte, , vol. 16, p. 1828
参考文献
Kumamoto pharm.Bl., , # 1 p. 54