反应条件
1: 87 percent / tert-butyl hypochlorite, triethylamine / 2-methyl-propan-2-ol; ethanol / 0.5 h / 0 °C 2: 1.) methyl iodide, 2.) 1N aq. NaOH / 1.) DMF, 60 deg C, 20 h, 2.) water, RT, 6 h View Scheme
参考文献
Hatanaka, Yasumaru; Nakayama, Hitoshi; Kanaoka, Yuichi
Heterocycles, 1993 , vol. 35, # 2 p. 997 - 1004