3,4-二甲氧基苯甲酰胺合成路线 (共 25 条)
反应条件
hydroxylamine hydrochloride in acetonitrile 0.0652778 h; Microwave irradiation;
参考文献
Datta, Bandita; Pasha
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 7 p. 2129 - 2130
反应条件
1: With NbCl5 in dichloromethane 2: With ammonia in dichloromethane T=45 - 50°C; 3 h;
参考文献
Nery, Marcelo S.; Ribeiro, Renata P.; Lopes, Claudio C.; Lopes, Rosangela S. C.
Synthesis, 2003 , # 2 p. 272 - 276
反应条件
anhydrous iron chloride; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; hydroxylamine hydrochloride; iodine; potassium carbonate in 1,2-dichloro-ethane T=90°C; 9 h;
参考文献
Das, Rima; Chakraborty, Debashis
Catalysis Communications, 2012 , vol. 26, p. 48 - 53
参考文献
Lempert-Sreter, M.; Lempert, K.; Tamas, J.; Vekey, K.
Acta Chimica Academiae Scientiarum Hungaricae, 1980 , vol. 103, # 2 p. 259 - 270
反应条件
oxygen; copper diacetate in acetic acid T=120°C; 10 h;
参考文献
Reddy, Mallu Chenna; Manikandan, Rajendran; Jeganmohan, Masilamani
Chemical Communications, 2013 , vol. 49, # 54 p. 6060 - 6062
反应条件
[η5-pentamethylcyclopentadienyl*Ir(H2O)3][OTf ]2 in water T=110°C; 12 h; Schlenk technique;
参考文献
Sun, Chunlou; Qu, Panpan; Li, Feng
Catalysis Science and Technology, 2014 , vol. 4, # 4 p. 988 - 996
反应条件
sodium azide; iodine; sodium hydrogencarbonate in water T=100°C; 2 h;
参考文献
Rajendar; Kant, Ruchir; Narender
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3591 - 3596
反应条件
copper(II)-modified 4Å molecular sieve in acetonitrile T=80°C; 8 h;
参考文献
Kiss, Arpad; Hell, Zoltan
Synthetic Communications, 2013 , vol. 43, # 13 p. 1778 - 1786
反应条件
sodium azide; [bis(acetoxy)iodo]benzene in acetonitrile T=0 - 80°C; 36 h; Inert atmosphere;
参考文献
Li, Xiao-Qiang; Wang, Wei-Kun; Han, Yi-Xin; Zhang, Chi
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 14-15 p. 2588 - 2598
反应条件
polyphosphoric acid containing 85percent P2O5 T=90 - 95°C; 5 h;
参考文献
Aksenov, Alexander V.; Aksenov, Nicolai A.; Nadein, Oleg N.; Aksenova, Inna V.
Synthetic Communications, 2012 , vol. 42, # 4 p. 541 - 547