in toluene (N2); a suspn. of Cu2O stirred with 1,5-cyclooctadiene; a soln. of F-compound added dropwise over a 30 min period; filtered; evapd.; elem. anal.;
参考文献
Doyle, G.; Eriksen, K. A.; Engen, D. Van
Organometallics, 1985 , vol. 4, p. 830 - 835
in further solvent(s) dissolving of Cu(CH3COO)2*H2O in anhyd. CF3COCH2COCF3; boiling for 5 min;; evapn. of the excess of diketone; recrystn. of the residue from CCl4;;
参考文献
Belford, R. L.; Martell, A. E.; Calvin, M.
J. inorg. nuclear Chem., 1956 , vol. 2, p. 11 - 31
in diethyl ether; water aq. soln. of copper acetate mixed with ether soln. of β-diketone; ether layer sepd.; repeated extd. (ether); ether exts. combined; dried (MgSO4); evapd.; ppt. recrustd. (2-3 times); IR; m.p.; elem.anal.;
参考文献
Kamalov, G. L.; Zheltvai, I. I.; Nekhoroshkov, V. P.; Mitkov, M. I.
Sov. Prog. Chem. (Engl. Transl.), 1982 , vol. 48/11, p. 21 - 25
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1982 , vol. 48/11, p. 1142 - 1147
in tetrachloromethane mixt. of freshly prepared Cu(OH)2 and acetylacetone in CCl4 boiled and standed overnight at room temp.; ppt. filtered, recrystd. (CHCl3), sublimed at 115-120°C, placed in a closed vessel over concd. H2SO4, elem. anal.;
参考文献
Fedotova, N. E.; Voityuk, A. A.; Bliznyuk, A. A.; Igumenov, I. K.
Sov. J. Coord. Chem. (Engl. Transl.), 1988 , vol. 14, p. 842 - 855
Koordinatsionnaya Khimiya, 1988 , vol. 14, p. 1493 - 1506
