反应条件
in dichloromethane stirring under slow stream of N2 for 24 h at room temp.; concn., chromy (alumina, CH2Cl2), separation of Co4(CO)12, W(CO)6 and NEt4(Co(CO)4), concn. of major eluate, CO bubbling through soln. for 10 min, trichloroethylene added, cooled to -20°C, elem. anal.;
参考文献
Baumann, Franz-Erich; Howard, Judith A. K.; Musgrove, Rupert J.; Sherwood, Paul; Stone, F. Gordon A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 1891 - 1898
